(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

Base Information

Chemical Name:(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane
CAS No.:208037-05-2
Molecular Formula:C₃₆H₄₂N₂O₂
Molecular Weight:534.742
Hs Code.:

Synonyms:(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

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Technology Process of (1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

There total 3 articles about (1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 20780-53-4
(R)-Styrene oxide

: 65838-10-0,135613-88-6,143443-23-6,191480-61-2
(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine

: 208037-05-2
(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

Guidance literature:: In methanol; at 40 - 60 ℃; for 72h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.10.020

Reference yield:

: 100-52-7
benzaldehyde

: 208037-05-2
(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol

1.2: Alkaline conditions

2.1: methanol

In methanol;
DOI:10.1016/j.tetasy.2016.05.009

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 208037-05-2
(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol

1.2: Alkaline conditions

2.1: methanol

In methanol;
DOI:10.1016/j.tetasy.2016.05.009