α-neopenyl chloride

Base Information

Chemical Name:α-neopenyl chloride
CAS No.:100702-94-1
Molecular Formula:C₁₁H₁₄ClNOS
Molecular Weight:243.757
Hs Code.:

α-<o-(N-sulfinylamino)phenyl>neopenyl chloride

Synonyms:α-neopenyl chloride

Suppliers and Price of α-neopenyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-neopenyl chloride

Chemical Property:

Purity/Quality:

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Technology Process of α-neopenyl chloride

There total 3 articles about α-neopenyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 100702-93-0
α-(o-aminophenyl)neopentyl alcohol

: 100702-94-1
α-neopenyl chloride

Guidance literature:: With thionyl chloride; In benzene; for 23h; Heating;
DOI:10.1021/jo00358a005

Reference yield:

: 525-76-8
2-methyl-4-oxo-3,1-benzoxazine

: 100702-94-1
α-neopenyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, 2.) aq. HCl / 1.) ether, benzene, 3 h, 2.) ether, benzene

2: 92 percent / KOH / methanol; H₂O / 23 h / Heating

3: 77 percent / thionyl chloride / benzene / 23 h / Heating

With hydrogenchloride; potassium hydroxide; thionyl chloride; magnesium; In methanol; water; benzene;
DOI:10.1021/jo00358a005

Reference yield:

: 100702-92-9
α-(o-acetamidophenyl)neopentyl alcohol

: 100702-94-1
α-neopenyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / KOH / methanol; H₂O / 23 h / Heating

2: 77 percent / thionyl chloride / benzene / 23 h / Heating

With potassium hydroxide; thionyl chloride; In methanol; water; benzene;
DOI:10.1021/jo00358a005