C₂₄H₃₆O₆

Base Information

Chemical Name:C₂₄H₃₆O₆
CAS No.:1352145-61-9
Molecular Formula:C₂₄H₃₆O₆
Molecular Weight:420.546
Hs Code.:

C<sub>24</sub>H<sub>36</sub>O<sub>6</sub>

Synonyms:C₂₄H₃₆O₆

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Chemical Property of C₂₄H₃₆O₆

Chemical Property:

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Technology Process of C₂₄H₃₆O₆

There total 7 articles about C₂₄H₃₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352145-60-8
(R)-(E)-4-(2-(methoxymethoxy) 3-(4-(methoxymethoxy)butyl)phenyl)but-3-en-2-yl-4-methylpent-3-enoate

: 1352145-61-9
C₂₄H₃₆O₆

: C₂₄H₃₆O₆

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; tert-butyldimethylsilyl chloride; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃; for 15h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol203060v

Reference yield:

: 1352145-56-2
C₁₈H₂₆O₅

: 1352145-61-9
C₂₄H₃₆O₆

: C₂₄H₃₆O₆

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

3: N,N,N,N,N,N-hexamethylphosphoric triamide; tert-butyldimethylsilyl chloride; lithium diisopropyl amide / tetrahydrofuran / 15 h / -78 - 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; di-isopropyl azodicarboxylate; tert-butyldimethylsilyl chloride; lithium diisopropyl amide; In tetrahydrofuran; methanol; 2: Mitsunobu reaction / 3: Ireland-Claisen rearrangement;
DOI:10.1021/ol203060v

Reference yield:

: 1352145-53-9
C₁₄H₂₂O₄

: 1352145-61-9
C₂₄H₃₆O₆

: C₂₄H₃₆O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butyl lithium / hexane; pentane / 2 h / 0 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / water / 6 h / 0 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

4.1: di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

5.1: N,N,N,N,N,N-hexamethylphosphoric triamide; tert-butyldimethylsilyl chloride; lithium diisopropyl amide / tetrahydrofuran / 15 h / -78 - 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; di-isopropyl azodicarboxylate; tert.-butyl lithium; tert-butyldimethylsilyl chloride; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; water; pentane; 2.1: Aldol condensation / 4.1: Mitsunobu reaction / 5.1: Ireland-Claisen rearrangement;
DOI:10.1021/ol203060v