{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

Base Information

Chemical Name:{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone
CAS No.:185686-48-0
Molecular Formula:C₂₉H₃₆O₄
Molecular Weight:448.602
Hs Code.:

Synonyms:{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

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Chemical Property of {3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

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Technology Process of {3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

There total 4 articles about {3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 66408-80-8,70238-39-0,80444-67-3,143590-48-1,38290-53-8
(2E,6E)-2,6-dimethyl-8-((tetrahydro-2H-pyran-2-yl)oxy)octa-2,6-dien-1-ol

: 22071-24-5
3-benzoylbenzyl bromide

: 185686-48-0
{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(96)02066-7

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 185686-48-0
{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium p-toluenesulfonate / CH₂Cl₂

2: 56 percent / t-BuOOH, H₂SeO₃, salicylic acid / CH₂Cl₂

3: 80 percent / NaH / tetrahydrofuran

With tert.-butylhydroperoxide; pyridinium p-toluenesulfonate; selenious acid; sodium hydride; salicylic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(96)02066-7

Reference yield:

: 59632-99-4
geranyl 2-tetrahydropyranyl ether

: 185686-48-0
{3-[(2E,6E)-2,6-Dimethyl-8-(tetrahydro-pyran-2-yloxy)-octa-2,6-dienyloxymethyl]-phenyl}-phenyl-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / t-BuOOH, H₂SeO₃, salicylic acid / CH₂Cl₂

2: 80 percent / NaH / tetrahydrofuran

With tert.-butylhydroperoxide; selenious acid; sodium hydride; salicylic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(96)02066-7