(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Base Information

Chemical Name:(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline
CAS No.:1434175-72-0
Molecular Formula:C₂₅H₂₈BrN₃O₄
Molecular Weight:514.419
Hs Code.:

Synonyms:(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Suppliers and Price of (E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

There total 4 articles about (E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.4%

: 24424-99-5
di-tert-butyl dicarbonate

: 1434175-70-8
(E)-4-[2-(6-bromo-1H-benzimidazol-2-yl)ethenyl]aniline

: 1434175-72-0
(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Guidance literature:: With guanidine hydrochloride; In ethanol; at 40 ℃; for 2h;
DOI:10.1016/j.bmc.2013.02.054

Reference yield:

: 1575-37-7
4-Bromo-benzene-1,2-diamine

: 1434175-72-0
(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium metabisulfite / N,N-dimethyl-formamide / 2 h / 105 °C

2: hydrogenchloride; iron / ethanol; water / 24 h / Reflux

3: guanidine hydrochloride / ethanol / 2 h / 40 °C

With hydrogenchloride; sodium metabisulfite; guanidine hydrochloride; iron; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.02.054

Reference yield:

: 1434175-67-3
(E)-6-bromo-2-(4-nitrostyryl)-1H-benzimidazole

: 1434175-72-0
(E)-4-[2-(6-bromo-1-tert-butoxycarbonylbenzimidazol-2-yl)ethenyl]-N-tert-butoxycarbonylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; iron / ethanol; water / 24 h / Reflux

2: guanidine hydrochloride / ethanol / 2 h / 40 °C

With hydrogenchloride; guanidine hydrochloride; iron; In ethanol; water;
DOI:10.1016/j.bmc.2013.02.054