(η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

Base Information

Chemical Name:(η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe
CAS No.:914613-79-9
Molecular Formula:C₂₄H₂₈FeN₂
Molecular Weight:400.347
Hs Code.:

Synonyms:(η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

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Chemical Property of (η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

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Technology Process of (η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

There total 1 articles about (η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1271-47-2
ferroceneacetylene

: 3,5-bis[(dimethylamino)methyl]phenyl iodide

: 914613-79-9
(η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

Guidance literature:: With CuI; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In neat (no solvent); under N2 atm. Fe complex, aryl iodide, (PdCl2(PPh3)2), and CuI were dissolved in i-Pr2NH and heated at reflux for 5 h; soln. was evapd. in vacuo, chromy. on alumina; elem. anal.;
DOI:10.1016/j.ica.2006.05.045

Reference yield: 80.0%

: 914613-79-9
(η5-C5H5)(η5-C5H4CCC6H3(CH2NMe2)2-3,5)Fe

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 914613-89-1
[(ferrocenyl)CC(C₆H₂I(CH₂NMe₂)2)]

Guidance literature:: With n-BuLi; In diethyl ether; under N2 atm. to soln. Fe complex in n-hexane soln. n-BuLi in n-hexane were added at 25°C and stirred for 16 h, volatiles were removed invacuo, residue was dissolved in Et2O, treated with I2 and stirred at 25 °C for 6 h; aq. soln. Na2S2O3 was added, org. phase was extd. with water, dried overMgSO4, filtered, and evapd. in vacuo; elem. anal.;
DOI:10.1016/j.ica.2006.05.045