(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

Base Information

Chemical Name:(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol
CAS No.:137676-01-8
Molecular Formula:C₁₈H₃₄O₂
Molecular Weight:282.467
Hs Code.:

Synonyms:(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

Suppliers and Price of (2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

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Technology Process of (2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

There total 2 articles about (2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 97536-46-4,122090-03-3
(2R,4S,6S,7S,10R)-7-Isopropyl-2,4,10-trimethyl-1,5-dioxa-spiro[5.5]undecane

: 762-72-1
allyl-trimethyl-silane

: 137676-01-8
(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -85 ℃; for 24h;
DOI:10.1246/cl.1990.1441

Reference yield:

: 10458-14-7,14073-97-3,17627-49-5,7786-64-3
(2R,5S)-menthone

: 121949-42-6
2,2,4,6,8,8-hexamethyl-3,7-dioxa-2,8-disilanonane

: 762-72-1
allyl-trimethyl-silane

: 137676-01-8
(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; titanium tetrachloride; Yield given. Multistep reaction; 1) CH₂Cl₂, -40 deg C, 18 h, 2) CH₂Cl₂, -85 deg C;
DOI:10.1246/cl.1990.1441

Reference yield:

: 137676-01-8
(2S,4R)-4-((1S,2S,5R)-1-Allyl-2-isopropyl-5-methyl-cyclohexyloxy)-pentan-2-ol

: 137765-97-0
(2R,4S)-4-benzyloxy-2-pentanol

Guidance literature:: Multi-step reaction with 2 steps

1: KN(SiMe₃)2 / tetrahydrofuran

2: 5percent CF₃COOH / CH₂Cl₂ / Ambient temperature

With potassium hexamethylsilazane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1246/cl.1990.1441