4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol

Base Information

• Chemical Name: 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol
• CAS No.: 69789-09-9
• Molecular Formula: C₂₁H₃₃NO₂
• Molecular Weight: 331.499

Synonyms:4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol

Chemical Property of 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol

Chemical Property:

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Technology Process of 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol

There total 4 articles about 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) → 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol (69789-09-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / PtO₂ / ethanol

2: Et₃N / benzene / 2.5 h / Heating

3: LiAlH₄ / benzene / 2.5 h / Heating

With lithium aluminium tetrahydride; hydrogen; triethylamine; platinum(IV) oxide; In ethanol; benzene;

DOI:10.1021/jm00353a016

Reference yield:

6-methoxy-2-tetralone (2472-22-2) → 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol (69789-09-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / PtO₂ / ethanol

2: Et₃N / benzene / 2.5 h / Heating

3: LiAlH₄ / benzene / 2.5 h / Heating

With lithium aluminium tetrahydride; hydrogen; triethylamine; platinum(IV) oxide; In ethanol; benzene;

DOI:10.1021/jm00353a016

Reference yield:

N-Cyclohexyl-N-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-succinamic acid methyl ester (69789-08-8) → 4-[Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amino]-butan-1-ol (69789-09-9)

Guidance literature:

With lithium aluminium tetrahydride; In benzene; for 2.5h; Heating;

DOI:10.1021/jm00353a016

upstream raw materials:

N-Cyclohexyl-N-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-succinamic acid methyl ester

Cyclohexyl-(6-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-amine

cyclohexylamine

6-methoxy-2-tetralone

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