2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

Base Information

Chemical Name:2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane
CAS No.:156910-36-0
Molecular Formula:C₂₅H₃₀O₂S₂
Molecular Weight:426.644
Hs Code.:

Synonyms:2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

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Chemical Property of 2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

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Technology Process of 2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

There total 4 articles about 2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 540-63-6
ethane-1,2-dithiol

: 117259-83-3
methyl 4-[(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)carbonyl]benzoate

: 156910-36-0
2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.5b01780

Reference yield: 90.0%

: 109-80-8
1.3-propanedithiol

: 117259-83-3
methyl 4-[(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)carbonyl]benzoate

: 156910-36-0
2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jm00017a021

Reference yield:

: 6683-46-1
1,1,4,4-Tetramethyl-1,2,3,4-tetrahydro-naphthalene

: 156910-36-0
2-(4-carbomethoxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)-1,3-dithiolane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / AlCl₃ / 1,2-dichloro-ethane / 16 h / Ambient temperature

2: 90 percent / BF₃*Et₂O / CH₂Cl₂ / 1 h / 0 °C

With aluminium trichloride; boron trifluoride diethyl etherate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm00017a021