2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

Base Information

Chemical Name:2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride
CAS No.:1449292-85-6
Molecular Formula:C₂₈H₃₈Cl₂CoN₄
Molecular Weight:560.536
Hs Code.:

Synonyms:2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

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Chemical Property of 2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

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Technology Process of 2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

There total 5 articles about 2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1449292-77-6
2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 1449292-85-6
2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.apcata.2013.04.026

Reference yield:

: 21190-88-5
6-bromopyridine-2-carboxylic acid ethyl ester

: 1449292-85-6
2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / 1,4-dioxane / Inert atmosphere; Reflux

2.1: sodium / ethanol; ethyl acetate / 5 h / Reflux

2.2: 4 h / Reflux

3.1: acetic acid / methanol / Reflux

4.1: tetrahydrofuran / 24 h / 20 °C

With potassium tert-butylate; sodium; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; ethyl acetate;
DOI:10.1016/j.apcata.2013.04.026

Reference yield:

: 1449292-69-6
ethyl 6-(3,5-diisopropylpyrazol-1-yl)pyridine-2-carboxylate

: 1449292-85-6
2-[1-(2,6-diisopropylphenylimino)ethyl]-6-(3,5-diisopropylpyrazol-1-yl)pyridine cobaltdichloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / ethanol; ethyl acetate / 5 h / Reflux

1.2: 4 h / Reflux

2.1: acetic acid / methanol / Reflux

3.1: tetrahydrofuran / 24 h / 20 °C

With sodium; acetic acid; In tetrahydrofuran; methanol; ethanol; ethyl acetate;
DOI:10.1016/j.apcata.2013.04.026