2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

Base Information

Chemical Name:2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine
CAS No.:195450-75-0
Molecular Formula:C₂₆H₃₂NPS
Molecular Weight:421.587
Hs Code.:

Synonyms:2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

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Chemical Property of 2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

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Technology Process of 2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

There total 5 articles about 2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3864-43-5
methanesulfonic acid 3-methyloxetan-3-ylmethyl ester

: 195450-75-0
2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / 2.5 M nBuLi / tetrahydrofuran; hexane / 12 h / Ambient temperature

2: 54 percent / H₂O / 120 h / 150 °C / 22501.8 Torr

3: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

4: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

With n-butyllithium; In tetrahydrofuran; hexane; water;
DOI:10.1002/cber.19971300917

Reference yield:

: 100-53-8
phenylmethanethiol

: 195450-75-0
2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / 2.5 M nBuLi / tetrahydrofuran; hexane / 12 h / Ambient temperature

2: 54 percent / H₂O / 120 h / 150 °C / 22501.8 Torr

3: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

4: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

With n-butyllithium; In tetrahydrofuran; hexane; water;
DOI:10.1002/cber.19971300917

Reference yield:

: 195450-63-6
2-Benzylsulfanylmethyl-3-dimethylamino-2-methyl-propan-1-ol

: 195450-75-0
2-(benzylsulfanylmethyl)-2-(diphenylphosphanylmethyl)-N,N-dimethylpropanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

2: 2.5 M nBuLi / hexane; tetrahydrofuran / Ambient temperature

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/cber.19971300917