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C49H48BF2N5O10

Base Information
  • Chemical Name:C49H48BF2N5O10
  • CAS No.:1234293-50-5
  • Molecular Formula:C49H48BF2N5O10
  • Molecular Weight:915.755
  • Hs Code.:
C<sub>49</sub>H<sub>48</sub>BF<sub>2</sub>N<sub>5</sub>O<sub>10</sub>

Synonyms:C49H48BF2N5O10

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Chemical Property of C49H48BF2N5O10
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Technology Process of C49H48BF2N5O10

There total 8 articles about C49H48BF2N5O10 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1021/bc100051p
Guidance literature:
Multi-step reaction with 6 steps
1.1: diethylamine / ethanol / 16 h / Reflux
2.1: ammonium acetate / ethanol / 24 h / Reflux
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16.33 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
5.3: 3 h / 20 °C
6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 16 h / 0 - 20 °C
With di-isopropyl azodicarboxylate; ammonium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; dmap; In tetrahydrofuran; ethanol; dichloromethane;
Guidance literature:
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 0 - 20 °C
With dmap; di-isopropyl azodicarboxylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/bc100051p
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