4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

Base Information

Chemical Name:4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide
CAS No.:473544-56-8
Molecular Formula:C₁₄H₂₀N₄O₄S₂
Molecular Weight:372.469
Hs Code.:

Synonyms:4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

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Chemical Property of 4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

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Technology Process of 4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

There total 6 articles about 4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135773-25-0
4-iodo-N,N-dimethyl-1H-imidazole-1-sulfonamide

: 473544-56-8
4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: EtMgBr / CH₂Cl₂; diethyl ether / 0.5 h

1.2: CH₂Cl₂; diethyl ether / 20 °C

2.1: 0.81 g / Et₃SiH; TFA / 16 h / Heating

3.1: 100 percent / H₂ / Pd/C / ethyl acetate / 16 h / 760 Torr

4.1: pyridine / CH₂Cl₂ / 20 °C

With pyridine; triethylsilane; ethylmagnesium bromide; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm030551a

Reference yield:

: 258528-27-7
4-[hydroxy(3-nitrophenyl)methyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

: 473544-56-8
4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.81 g / Et₃SiH; TFA / 16 h / Heating

2: 100 percent / H₂ / Pd/C / ethyl acetate / 16 h / 760 Torr

3: pyridine / CH₂Cl₂ / 20 °C

With pyridine; triethylsilane; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm030551a

Reference yield:

: 473544-55-7
4-(3-nitrobenzyl)imidazole-1-sulfonic acid dimethylamide

: 473544-56-8
4-(3-ethanesulfonylamino-benzyl)-imidazole-1-sulfonic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethyl acetate / 16 h / 760 Torr

2: pyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm030551a