1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

Base Information

Chemical Name:1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene
CAS No.:296761-59-6
Molecular Formula:C₂₉H₄₈OSi₂
Molecular Weight:468.871
Hs Code.:

Synonyms:1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

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Technology Process of 1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

There total 3 articles about 1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 296761-57-4
1-Bromo-3-hexyloxymethyl-5-triisopropylsilylethynylbenzene

: 1066-54-2
trimethylsilylacetylene

: 296761-59-6
1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

Guidance literature:: With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 80 ℃; for 24h;
DOI:10.1002/1521-3765(20000703)6:13<2362::AID-CHEM2362>3.0.CO;2-G

Reference yield:

: 89343-06-6
tris-iso-propylsilyl acetylene

: 296761-59-6
1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / CuI; Et₃N / Pd(PPh₃)4 / 24 h / 60 °C

2: 97 percent / CuI; Et₃N / Pd(PPh₃)4 / 24 h / 80 °C

With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1: Substitution / 2: Substitution;
DOI:10.1002/1521-3765(20000703)6:13<2362::AID-CHEM2362>3.0.CO;2-G

Reference yield:

: 223463-19-2
1-Bromo-3-hexyloxymethyl-5-iodobenzene

: 296761-59-6
1-Hexyloxymethyl-3-triisopropylsilylethynyl-5-trimethylsilylethynylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / CuI; Et₃N / Pd(PPh₃)4 / 24 h / 60 °C

2: 97 percent / CuI; Et₃N / Pd(PPh₃)4 / 24 h / 80 °C

With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1: Substitution / 2: Substitution;
DOI:10.1002/1521-3765(20000703)6:13<2362::AID-CHEM2362>3.0.CO;2-G