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C42H53NO6Si

Base Information Edit
C<sub>42</sub>H<sub>53</sub>NO<sub>6</sub>Si

Synonyms:C42H53NO6Si

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C42H53NO6Si Edit
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Technology Process of C42H53NO6Si

There total 10 articles about C42H53NO6Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 120h;
Guidance literature:
Multi-step reaction with 9 steps
1.1: tetrakis(triphenylphosphine) palladium(0); 1-amino-2-propene; 1,3-dimethylbarbituric acid / dichloromethane / 2 h / 40 °C / Inert atmosphere
2.1: potassium carbonate / acetonitrile / 18 h / Reflux
3.1: zinc; ammonium chloride / acetone; water / 4.5 h / 60 °C
4.1: caesium carbonate / tetrahydrofuran / 70 °C
5.1: palladium diacetate; 1,3-bis-(diphenylphosphino)propane; triethylsilane / tetrahydrofuran / 20 °C
6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - -10 °C
6.2: -78 - 20 °C
7.1: boron tribromide / dichloromethane / 0.25 h / 0 °C
8.1: toluene-4-sulfonic acid / benzene / 1 h / Reflux; Dean-Stark
9.1: 1H-imidazole / N,N-dimethyl-formamide / 120 h / 20 °C
With 1H-imidazole; triethylsilane; tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; sodium hexamethyldisilazane; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; toluene-4-sulfonic acid; 1-amino-2-propene; zinc; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; benzene;
Guidance literature:
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / benzene / 1 h / Reflux; Dean-Stark
2: 1H-imidazole / N,N-dimethyl-formamide / 120 h / 20 °C
With 1H-imidazole; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; benzene;
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