Technology Process of C42H53NO6Si
There total 10 articles about C42H53NO6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 120h;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: tetrakis(triphenylphosphine) palladium(0); 1-amino-2-propene; 1,3-dimethylbarbituric acid / dichloromethane / 2 h / 40 °C / Inert atmosphere
2.1: potassium carbonate / acetonitrile / 18 h / Reflux
3.1: zinc; ammonium chloride / acetone; water / 4.5 h / 60 °C
4.1: caesium carbonate / tetrahydrofuran / 70 °C
5.1: palladium diacetate; 1,3-bis-(diphenylphosphino)propane; triethylsilane / tetrahydrofuran / 20 °C
6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - -10 °C
6.2: -78 - 20 °C
7.1: boron tribromide / dichloromethane / 0.25 h / 0 °C
8.1: toluene-4-sulfonic acid / benzene / 1 h / Reflux; Dean-Stark
9.1: 1H-imidazole / N,N-dimethyl-formamide / 120 h / 20 °C
With
1H-imidazole; triethylsilane; tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; sodium hexamethyldisilazane; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; toluene-4-sulfonic acid; 1-amino-2-propene; zinc;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / benzene / 1 h / Reflux; Dean-Stark
2: 1H-imidazole / N,N-dimethyl-formamide / 120 h / 20 °C
With
1H-imidazole; toluene-4-sulfonic acid;
In
N,N-dimethyl-formamide; benzene;