4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide

Base Information

• Chemical Name: 4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide
• CAS No.: 1180530-22-6
• Molecular Formula: C₂₁H₂₂N₆O₂S
• Molecular Weight: 422.511

Synonyms:4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide

Chemical Property of 4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide

Chemical Property:

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Technology Process of 4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide

There total 1 articles about 4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-[3-cyano-4-(4-dimethylsulfamoyl-phenyl)-1-p-tolyl-1H-pyrrol-2-yl]formimidic acid ethyl ester (1180530-16-8) → 4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide (1180530-22-6)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 7h;

DOI:10.1080/10426500802111207

Reference yield: 92.0%

4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide (1180530-22-6) + oxalic acid (144-62-7,97993-78-7) → 7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]pyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine (1180530-23-7)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; for 8h; Reflux;

DOI:10.1080/10426500802111207

Reference yield: 82.0%

4-(3-amino-4-imino-7-p-tolyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)-N,N-dimethylbenzenesulfonamide (1180530-22-6) + diethyl malonate (105-53-3) → 2-ethoxycarbonylmethyl-7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]pyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine (1180530-28-2)

Guidance literature:

In ethanol; for 5h; Reflux;

DOI:10.1080/10426500802111207

upstream raw materials:

N-[3-cyano-4-(4-dimethylsulfamoyl-phenyl)-1-p-tolyl-1H-pyrrol-2-yl]formimidic acid ethyl ester

Downstream raw materials:

2-thioxo-7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]-2,3-dihydropyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine

7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]pyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine

2-methyl-7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]pyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine

2-phenyl-7-p-tolyl-9-[4-(N,N-dimethylaminosulfonylphenyl)]pyrrolo[3,2-e][1,2,4]triazolo[1,5-c]pyrimidine

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