5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

Base Information

Chemical Name:5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)
CAS No.:1196870-89-9
Molecular Formula:C₃₇H₄₅N₂O₈PS₂Si
Molecular Weight:768.964
Hs Code.:

Synonyms:5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

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Technology Process of 5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

There total 1 articles about 5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.4%

: 1196870-90-2
C₃₇H₄₅N₂O₇PS₂Si

: 1196870-89-9
5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

Guidance literature:: With tert.-butylhydroperoxide; In decane; benzene; at 20 ℃;
DOI:10.1080/10426500902947898

Reference yield:

: 1196870-89-9
5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

: 74925-81-8
N²-isobutyryl-3'-O-acetyl-2'-deoxyguanosine

: C₅₁H₆₂N₇O₁₄PSSi

: C₅₁H₆₂N₇O₁₄PSSi

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 2h; optical yield given as %de;
DOI:10.1080/10426500902947898

Reference yield:

: 1196870-89-9
5'-O-monomethoxytrityl-2'-O-tert-butyldimethylsilyluridine-3'-O-(2-oxo-1,3,2-dithiaphospholane)

: 9-(2',3'-di-O-acetyl-β-D-ribofuranosyl)-N2-isobutanoylguanine

: C₅₃H₆₄N₇O₁₆PSSi

: C₅₃H₆₄N₇O₁₆PSSi

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 2h; optical yield given as %de;
DOI:10.1080/10426500902947898