{Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄

Base Information

• Chemical Name: {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄
• CAS No.: 90442-61-8
• Molecular Formula: C₃₃H₃₁N₆OPRh*ClO₄
• Molecular Weight: 760.979

Synonyms:{Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄

Chemical Property of {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄

Chemical Property:

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Technology Process of {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄

There total 2 articles about {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

{Rh(tetrafluorobenzobarrelene)(3,6-bis(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO4 (90443-75-7) → {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO4 (90442-61-8)

Guidance literature:

With CO; PPh₃; In dichloromethane; CO bubbled through soln. of Rh complex for 60 min, added triphenylphosphine (molar ratio 1:1); concd. in vac., pptd. with ether, filtered off, washed with ether, air-dried, elem. anal.;

DOI:10.1016/S0277-5387(00)88052-3

Reference yield:

3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine (29334-74-5) → {Rh(carbon monoxide)(triphenylphosphine)(3,6-bis-(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO4 (90442-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: CO; PPh₃ / dichloromethane

With CO; PPh₃; In dichloromethane; acetone;

DOI:10.1016/S0277-5387(00)88052-3

upstream raw materials:

{Rh(tetrafluorobenzobarrelene)(3,6-bis(3,5-dimethylpyrazol-1-yl)pyridazine)}ClO₄

3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

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