3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

Base Information

Chemical Name:3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine
CAS No.:29334-74-5
Molecular Formula:C₁₄H₁₆N₆
Molecular Weight:268.321
Hs Code.:
DSSTox Substance ID:DTXSID70570407
Nikkaji Number:J654.234D
Wikidata:Q82457827
Mol file:29334-74-5.mol

Synonyms:3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine;29334-74-5;DTXSID70570407;3,6-bis(3,5-dimethylpyrazol-1-yl)pyridazine

Suppliers and Price of 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:268.14364454
Heavy Atom Count:20
Complexity:306

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NN1C2=NN=C(C=C2)N3C(=CC(=N3)C)C)C

Technology Process of 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

There total 1 articles about 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30169-25-6
3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine

: N-ethyl-5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo-[3,2-b] carbazol-2-amine

: N-[6-(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine-3-yl]-N-ethyl-5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo [3,2-b]-carbazol-2-amine

: N-[6-(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine-3-yl]-5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazol-2-amine

: 29334-74-5
3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

Guidance literature:: In 1,3,5-trimethyl-benzene; for 13h; Reflux;
DOI:10.1007/s11172-021-3191-6

Reference yield: 89.0%

: 154790-97-3
[(η⁶-benzene)RuCl2(acetonitrile)]

: 75-09-2
dichloromethane

: 143-66-8
sodium tetraphenyl borate

: 29334-74-5
3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

: [RuCl(benzene)(3,6-bis(3,5-dimethylpyrazol-1-yl)pyridazine)]B(C₆H₅)4

Guidance literature:: In dichloromethane; N2, stoich., to a suspn. of Ru comd. added N compd., stirred at room temp. for 12 h, B compd. added, stirred for 1 h; sovent evapd., washed (CH2Cl2), recrystd. (CH2Cl2/pentane); elem. anal.;
DOI:10.1016/j.ica.2009.04.011

Reference yield: 87.0%

: 75-09-2
dichloromethane

: 81780-17-8
[Cu(MeCN)4]OTs

: 29334-74-5
3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine

: [Cu(3,6-bis(3,5-dimethylpyrazol-1-yl)pyridazine)]4(p-toluenesulfonate)4*2dichloromethane

Guidance literature:: In dichloromethane; byproducts: CH3CN; (N2); mixing CH2Cl2 solns. of copper compd. and pyridazine deriv., stirring at room temp. for 1 h; concg., addn. of diethyl ether, filtration, washing with ether, drying in vac. at room temp., recrystn. by pptn. with pentane from CH2Cl2 soln.,elem. anal.;
DOI:10.1021/ic701117a