cyclohexanecarboxyl diphenyl methyl silane

Base Information

Chemical Name:cyclohexanecarboxyl diphenyl methyl silane
CAS No.:122131-74-2
Molecular Formula:C₂₀H₂₄OSi
Molecular Weight:308.495
Hs Code.:

Synonyms:cyclohexanecarboxyl diphenyl methyl silane

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Chemical Property of cyclohexanecarboxyl diphenyl methyl silane

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Technology Process of cyclohexanecarboxyl diphenyl methyl silane

There total 2 articles about cyclohexanecarboxyl diphenyl methyl silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1172-76-5
1,2-dimethyl-1,1,2,2-tetraphenyldisilane

: 2719-27-9
cyclohexanylcarbonyl chloride

: 122131-74-2
cyclohexanecarboxyl diphenyl methyl silane

Guidance literature:: With vanadium(III) chloride; In tetrahydrofuran; at -70 ℃; for 1.33333h;
DOI:10.1016/0022-328X(88)80634-X

Reference yield:

: 144-79-6
chloromethyldiphenylsilane

: 122131-74-2
cyclohexanecarboxyl diphenyl methyl silane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / graphite, K / tetrahydrofuran / 0.08 h / 0 °C

2: 80 percent / C₈K, VCl₃ / tetrahydrofuran / 1.33 h / -70 °C

With vanadium(III) chloride; pyrographite; In tetrahydrofuran;
DOI:10.1016/0022-328X(88)80634-X

Reference yield:

: 122131-74-2
cyclohexanecarboxyl diphenyl methyl silane

: 105-36-2
ethyl bromoacetate

: 136578-52-4
ethyl 3-cyclohexyl-3-hydroxy-3-(diphenylmethylsilyl)propanoate

Guidance literature:: With silver graphite; silver(I) acetate; zinc(II) chloride; zinc; Yield given. Multistep reaction; 1.) THF, -40 deg C, 30 min, 2.) THF, RT, 2 h;
DOI:10.1016/0022-328X(91)86327-M