1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

Base Information

Chemical Name:1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate
CAS No.:1333114-57-0
Molecular Formula:C₂HF₃O₂*C₁₇H₁₉Br₂NO
Molecular Weight:527.176
Hs Code.:

Synonyms:1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

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Chemical Property of 1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

Chemical Property:

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Technology Process of 1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

There total 10 articles about 1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1333114-55-8
tert-butyl (1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-yl)carbamate

: 76-05-1
trifluoroacetic acid

: 1333114-57-0
1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

Guidance literature:: In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 1333114-57-0
1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / chloroform / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

2.2: 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

4.1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 2.33 h / 0 - 20 °C

5.1: dichloromethane / 2 h / 0 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; triphenylphosphine; dibenzoyl peroxide; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; mineral oil;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1333114-57-0
1-((2-(bromomethyl)benzyl)oxy)-3-(4-bromophenyl)propan-2-amine trifluoroacetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / 70 °C

2.1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

3.2: 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

5.1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 2.33 h / 0 - 20 °C

6.1: dichloromethane / 2 h / 0 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; triphenylphosphine; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane; diethyl ether; dichloromethane; mineral oil;