E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

Base Information

Chemical Name:E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester
CAS No.:118129-30-9
Molecular Formula:C₂₆H₂₇NO₂
Molecular Weight:385.506
Hs Code.:

Synonyms:E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

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Chemical Property of E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

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Technology Process of E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

There total 1 articles about E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1530-45-6
(carbethoxymethyl)triphenylphosphonium bromide

: 6,6-Dimethyl-2,3-diphenyl-6,7-dihydro-5H-pyrrolizine-1-carbaldehyde

: Z-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

: 118129-30-9
E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

Guidance literature:: With sodium ethanolate; In ethanol; dichloromethane; for 120h; Ambient temperature;
DOI:10.1002/ardp.19883210911

Reference yield: 82.0%

: 118129-30-9
E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

: 118129-34-3
E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeure

Guidance literature:: With potassium hydroxide; In ethanol; for 1h; Heating;
DOI:10.1002/ardp.19883210911

Reference yield:

: 118129-30-9
E-3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-acrylsaeureethylester

: 3-(2,2-Dimethyl-5,6-diphenyl-2,3-dihydro-1H-pyrrolizin-7-yl)-propionsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 10percent aq. KOH / ethanol / 1 h / Heating

2: 89 percent / H₂ / PtO₂ / tetrahydrofuran; ethanol / 4 h / 7500.6 Torr

With potassium hydroxide; hydrogen; platinum(IV) oxide; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.19883210911