methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate

Base Information

• Chemical Name: methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate
• CAS No.: 1012330-91-4
• Molecular Formula: C₂₆H₂₀N₂O₅
• Molecular Weight: 440.455

Synonyms:methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate

Chemical Property of methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate

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Technology Process of methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate

There total 1 articles about methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methyl 6-(2-(1-hydroxy-3-(4'-(hydroxymethyl)biphenyl-4-yl)propyl)oxazol-5-yl)pyridine-2-carboxylate (1012330-88-9) → methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate (1012330-91-4)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.583333h;

DOI:10.1021/jm701210y

Reference yield: 75.0%

pyrrolidine (123-75-1) + methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate (1012330-91-4) → 6-{2-[3-(4'-pyrrolidin-1-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester (1012329-68-8)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 3h;

DOI:10.1021/jm701210y

Reference yield: 64.0%

piperidine (110-89-4) + methyl 6-(2-(3-(4'-formylbiphenyl-4-yl)propanoyl)oxazol-5-yl)pyridine-2-carboxylate (1012330-91-4) → 6-{2-[3-(4'-piperidin-1-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester (1012329-67-7)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

DOI:10.1021/jm701210y

upstream raw materials:

methyl 6-(2-(1-hydroxy-3-(4'-(hydroxymethyl)biphenyl-4-yl)propyl)oxazol-5-yl)pyridine-2-carboxylate

Downstream raw materials:

6-{2-[3-(4'-pyrrolidin-1-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester

6-{2-[3-(4'-piperidin-1-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester

6-{2-[3-(4'-morpholin-4-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester

6-{2-[3-(4'-thiomorpholin-4-ylmethyl-biphenyl-4-yl)-propionyl]-oxazol-5-yl}-pyridine-2-carboxylic acid methyl ester

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