(E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

Base Information

Chemical Name:(E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate
CAS No.:1107608-22-9
Molecular Formula:C₃₅H₅₂O₈Si
Molecular Weight:628.879
Hs Code.:

Synonyms:(E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

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Chemical Property of (E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

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Technology Process of (E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

There total 1 articles about (E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1146896-66-3
C₃₉H₆₂O₁₀SSi

: 1107608-22-9
(E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In Dichlorofluoromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2008.10.059

Reference yield: 99.0%

: 1107608-22-9
(E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate

: 1107608-23-0
(E)-(4R,5R,11R)-5-(tert-butyldiphenylsilyloxy)-11-hydroxy-4-((2-methoxyethoxy)methoxy)-2-dodecenoic acid

Guidance literature:: (E)-(4R,5R,11R)-methyl 11-acetoxy-5-(tert-butyldiphenylsilyloxy)-4-((2-methoxyethoxy)methoxy)-2-dodecenoate; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 16h;

With hydrogenchloride; In tetrahydrofuran; water; pH=4;
DOI:10.1016/j.tet.2008.10.059