C₃₇H₃₅ClFN₃O₇S

Base Information

Chemical Name:C₃₇H₃₅ClFN₃O₇S
CAS No.:1234779-91-9
Molecular Formula:C₃₇H₃₅ClFN₃O₇S
Molecular Weight:720.218
Hs Code.:

C<sub>37</sub>H<sub>35</sub>ClFN<sub>3</sub>O<sub>7</sub>S

Synonyms:C₃₇H₃₅ClFN₃O₇S

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Chemical Property of C₃₇H₃₅ClFN₃O₇S

Chemical Property:

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Technology Process of C₃₇H₃₅ClFN₃O₇S

There total 19 articles about C₃₇H₃₅ClFN₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 217314-44-8
2-fluoro-6-iodo-4-methylaniline

: 1234779-91-9
C₃₇H₃₅ClFN₃O₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine

2.1: copper(l) iodide / N,N-dimethyl-formamide / 100 °C

3.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 15 °C

3.2: 20 °C

4.1: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 5 - 22 °C

5.1: tetrahydrofuran / 1 h / 40 °C / Inert atmosphere

6.1: tetrahydrofuran / 1.4 h / 60 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1.1: |Sonogashira Cross-Coupling;
DOI:10.1021/op300249q

Reference yield:

: 452-80-2
2-fluoro-4-methylaniline

: 1234779-91-9
C₃₇H₃₅ClFN₃O₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: aluminum (III) chloride; boron trichloride; sodium hydroxide / dichloromethane; water / 14 h / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / water; pentan-1-ol / 2.42 h / 20 °C / Reflux

3.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 15 °C

3.2: 20 °C

4.1: boron trifluoride diethyl etherate / dichloromethane / 22 °C

5.1: tetrahydrofuran / 1 h / 40 °C / Inert atmosphere

6.1: tetrahydrofuran / 1.4 h / 60 °C

With aluminum (III) chloride; sodium tetrahydroborate; boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate; boron trichloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; pentan-1-ol; water; toluene;
DOI:10.1021/op300249q

Reference yield:

: 2-fluoro-4-methyl-6-((trimethylsilyl)ethynyl)aniline

: 1234779-91-9
C₃₇H₃₅ClFN₃O₇S

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide / N,N-dimethyl-formamide / 100 °C

2.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 15 °C

2.2: 20 °C

3.1: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 5 - 22 °C

4.1: tetrahydrofuran / 1 h / 40 °C / Inert atmosphere

5.1: tetrahydrofuran / 1.4 h / 60 °C

With copper(l) iodide; boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/op300249q