C₂₄H₁₈FN

Base Information

Chemical Name:C₂₄H₁₈FN
CAS No.:1445138-70-4
Molecular Formula:C₂₄H₁₈FN
Molecular Weight:339.412
Hs Code.:

Synonyms:C₂₄H₁₈FN

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Chemical Property of C₂₄H₁₈FN

Chemical Property:

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Technology Process of C₂₄H₁₈FN

There total 3 articles about C₂₄H₁₈FN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1401560-11-9
2-((4-fluorophenyl)ethynyl)-N,N-dimethylaniline

: 766-97-2
4-n-methylphenylacetylene

: 1445138-70-4
C₂₄H₁₈FN

Guidance literature:: With palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid; In dimethyl sulfoxide; at 80 ℃; for 52h;
DOI:10.1002/chem.201403612

Reference yield:

: 766-98-3
1-ethynyl-4-fluorobenzene

: 1445138-70-4
C₂₄H₁₈FN

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 12 h / 20 °C / Inert atmosphere

2: palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / dimethyl sulfoxide / 24 h / 80 °C / 760.05 Torr

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine; In dimethyl sulfoxide;
DOI:10.1002/anie.201205596

Reference yield:

: 698-02-2
N,N-dimethyl-o-iodoaniline

: 1445138-70-4
C₂₄H₁₈FN

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 12 h / 20 °C / Inert atmosphere

2: palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / dimethyl sulfoxide / 24 h / 80 °C / 760.05 Torr

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine; In dimethyl sulfoxide;
DOI:10.1002/anie.201205596