Z-Lys-D-Trp-3-methylbutylamide hydrochloride

Base Information

• Chemical Name: Z-Lys-D-Trp-3-methylbutylamide hydrochloride
• CAS No.: 128684-46-8
• Molecular Formula: C₃₀H₄₁N₅O₄*ClH
• Molecular Weight: 572.148

Synonyms:Z-Lys-D-Trp-3-methylbutylamide hydrochloride

Chemical Property of Z-Lys-D-Trp-3-methylbutylamide hydrochloride

Chemical Property:

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Technology Process of Z-Lys-D-Trp-3-methylbutylamide hydrochloride

There total 3 articles about Z-Lys-D-Trp-3-methylbutylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Z-Lys(Boc)-D-Trp-isoamylamide (128684-45-7) → Z-Lys-D-Trp-3-methylbutylamide hydrochloride (128684-46-8)

Guidance literature:

With hydrogenchloride; acetic acid;

DOI:10.1021/jm00171a034

Reference yield:

Z-Lys(Boc)-OH (2389-60-8) → Z-Lys-D-Trp-3-methylbutylamide hydrochloride (128684-46-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), triethylamine / dimethylformamide

2: 96 percent / 3N HCl, AcOH

With hydrogenchloride; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1021/jm00171a034

Reference yield:

D-Trp-isoamylamide hydrochloride (128684-44-6) → Z-Lys-D-Trp-3-methylbutylamide hydrochloride (128684-46-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), triethylamine / dimethylformamide

2: 96 percent / 3N HCl, AcOH

With hydrogenchloride; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1021/jm00171a034

upstream raw materials:

Z-Lys(Boc)-D-Trp-isoamylamide

Z-Lys(Boc)-OH

D-Trp-isoamylamide hydrochloride

Downstream raw materials:

(R)-2-(4-{(S)-5-Benzyloxycarbonylamino-5-[(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-4-phenyl-butyrylamino)-3-phenyl-propionic acid methyl ester

(R)-2-(4-{(S)-5-Amino-5-[(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-4-phenyl-butyrylamino)-3-phenyl-propionic acid

(2R,5S)-2-Benzyl-3,11,15-trioxo-12-phenyl-1,4,10-triaza-cyclopentadecane-5-carboxylic acid [(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethyl]-amide

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