Z-Lys(Boc)-D-Trp-isoamylamide

Base Information

Chemical Name:Z-Lys(Boc)-D-Trp-isoamylamide
CAS No.:128684-45-7
Molecular Formula:C₃₅H₄₉N₅O₆
Molecular Weight:635.804
Hs Code.:

Synonyms:Z-Lys(Boc)-D-Trp-isoamylamide

Suppliers and Price of Z-Lys(Boc)-D-Trp-isoamylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-Lys(Boc)-D-Trp-isoamylamide

Chemical Property:

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Technology Process of Z-Lys(Boc)-D-Trp-isoamylamide

There total 1 articles about Z-Lys(Boc)-D-Trp-isoamylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2389-60-8
Z-Lys(Boc)-OH

: 128684-44-6
D-Trp-isoamylamide hydrochloride

: 128684-45-7
Z-Lys(Boc)-D-Trp-isoamylamide

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00171a034

Reference yield: 96.0%

: 128684-45-7
Z-Lys(Boc)-D-Trp-isoamylamide

: 128684-46-8
Z-Lys-D-Trp-3-methylbutylamide hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid;
DOI:10.1021/jm00171a034

Reference yield:

: 128684-45-7
Z-Lys(Boc)-D-Trp-isoamylamide

: 128684-15-1
(2R,5S)-2-Benzyl-3,11,15-trioxo-12-phenyl-1,4,10-triaza-cyclopentadecane-5-carboxylic acid [(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / 3N HCl, AcOH

2: 62 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), triethylamine / dimethylformamide

3: 2N aq. NaOH / methanol

4: H₂ / 5percent Pd-C / aq. ethanol

5: 17 percent / diphenyl phosphorazidate, NaHCO₃ / dimethylformamide

With hydrogenchloride; sodium hydroxide; diphenyl phosphoryl azide; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00171a034