3-cyanophenyl cycanate

Base Information

• Chemical Name: 3-cyanophenyl cycanate
• CAS No.: 52805-52-4
• Molecular Formula: C₈H₄N₂O
• Molecular Weight: 144.133

Synonyms:3-cyanophenyl cycanate

Chemical Property of 3-cyanophenyl cycanate

Chemical Property:

Purity/Quality:

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Technology Process of 3-cyanophenyl cycanate

There total 1 articles about 3-cyanophenyl cycanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromocyane (506-68-3) + m-cyanophenol (873-62-1) → 3-cyanophenyl cycanate (52805-52-4)

Guidance literature:

With triethylamine; In diethyl ether; at -10 ℃;

Reference yield: 70.0%

3-cyanophenyl cycanate (52805-52-4) + tert-butyl 1-(4-(4-amino-1-(4-aminobutyl)-2-butyl-1H-imidazo[4,5-c]quinolin-8-yl)piperazin-1-yl)-3,6,9,12,15,18,21,24,27,30,33,36,39,42,45,48,51,54,57,60,63,66,69,72-tetracosaoxapentaheptacontan-75-oate → tert-butyl 1-(4-(4-amino-2-butyl-1-(4-(3-(3-cyanophenyl)ureido)butyl)-1H-imidazo[4,5-c]quinolin-8-yl)piperazin-1-yl)-3,6,9,12,15,18,21,24,27,30,33,36,39,42,45,48,51,54,57,60,63,66,69,72-tetracosaoxapentaheptacontan-75-oate

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 16h; Sealed tube;

Reference yield:

3-cyanophenyl cycanate (52805-52-4) + phenyl isocyanate (103-71-9) + diethylamine (109-89-7) → C19H20N4O2 (52805-61-5)

Guidance literature:

Multistep reaction; (i) Et₂O, (ii) /BRN= 471391/;

upstream raw materials:

bromocyane

m-cyanophenol

Downstream raw materials:

C₁₉H₂₀N₄O₂

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