4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde

Base Information

• Chemical Name: 4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde
• CAS No.: 1318689-73-4
• Molecular Formula: C₃₆H₂₄F₃NO₃S
• Molecular Weight: 607.653
• Mol file: 1318689-73-4.mol

Synonyms:4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde

Chemical Property of 4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde

There total 1 articles about 4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

4-dibromo-2-(trifluoromethyl)benzaldehyde (211796-64-4,861928-27-0) + 2-tributylstannyl-5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophene → 4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde (1318689-73-4)

Guidance literature:

With trans-bis(triphenylphosphine)palladium dichloride; In N,N-dimethyl-formamide; at 90 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c1jm10107b

Reference yield: 55.0%

4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)benzaldehyde (1318689-73-4) + cyanoacetic acid (372-09-8) → (E)-3-(4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)phenyl)cyanoacrylic acid (1318689-64-3)

Guidance literature:

With ammonium acetate; In acetic acid; at 120 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c1jm10107b

upstream raw materials:

4-dibromo-2-(trifluoromethyl)benzaldehyde

Downstream raw materials:

(E)-3-(4-(5-(p-(naphthylphenylamino)phenyl)-3,4-ethylenedioxythiophen-2-yl)-2-(trifluoromethyl)phenyl)cyanoacrylic acid