Technology Process of dihydrofluoresceylhomoveratrylamide
There total 4 articles about dihydrofluoresceylhomoveratrylamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium dihydroxide;
In
ethyl acetate;
for 0.5h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 97 percent / NaBH4 / methanol / 1 h / Ambient temperature
2: 98 percent / K2CO3 / dimethylformamide / 3 h / 80 - 90 °C
3: 61.5 percent / 20percent aq. NaOH / ethanol / 2 h / Heating
4: 42 percent / DCC, dimethylaminopyridine / CH2Cl2 / 18 h / Ambient temperature
5: 75 percent / H2 / Pd(OH)2/C / ethyl acetate / 0.5 h / Ambient temperature
With
dmap; sodium hydroxide; sodium tetrahydroborate; hydrogen; potassium carbonate; dicyclohexyl-carbodiimide;
palladium dihydroxide;
In
methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 61.5 percent / 20percent aq. NaOH / ethanol / 2 h / Heating
2: 42 percent / DCC, dimethylaminopyridine / CH2Cl2 / 18 h / Ambient temperature
3: 75 percent / H2 / Pd(OH)2/C / ethyl acetate / 0.5 h / Ambient temperature
With
dmap; sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide;
palladium dihydroxide;
In
ethanol; dichloromethane; ethyl acetate;
