C₁₈H₁₆IN

Base Information

Chemical Name:C₁₈H₁₆IN
CAS No.:1260147-09-8
Molecular Formula:C₁₈H₁₆IN
Molecular Weight:373.236
Hs Code.:

Synonyms:C₁₈H₁₆IN

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Chemical Property of C₁₈H₁₆IN

Chemical Property:

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Technology Process of C₁₈H₁₆IN

There total 3 articles about C₁₈H₁₆IN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 828-80-8
1,2-dimethyl-5-phenyl-1H-pyrrole

: BF₄⁽¹⁺⁾*C₁₂H₈I₃⁽¹⁺⁾

: 1260147-09-8
C₁₈H₁₆IN

Guidance literature:: 1,2-dimethyl-5-phenyl-1H-pyrrole; With dichloro bis(acetonitrile) palladium(II); In 1,2-dichloro-ethane; at 20 ℃; for 0.0833333h;

BF₄⁽¹⁺⁾*C₁₂H₈I₃⁽¹⁺⁾; In 1,2-dichloro-ethane; at 84 ℃; for 2h;
DOI:10.1021/ol102734g

Reference yield:

: 5122-99-6
4-iodophenylboronic acid

: 1260147-09-8
C₁₈H₁₆IN

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid / diethyl ether; dichloromethane

2.1: dichloro bis(acetonitrile) palladium(II) / 1,2-dichloro-ethane / 0.08 h / 20 °C

2.2: 2 h / 84 °C

With dichloro bis(acetonitrile) palladium(II); boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol102734g

Reference yield:

: 583-05-1
1-phenylpentane-1,4-dione

: 1260147-09-8
C₁₈H₁₆IN

Guidance literature:: Multi-step reaction with 2 steps

1.1: aminosulfonic acid / ethanol

2.1: dichloro bis(acetonitrile) palladium(II) / 1,2-dichloro-ethane / 0.08 h / 20 °C

2.2: 2 h / 84 °C

With dichloro bis(acetonitrile) palladium(II); aminosulfonic acid; In ethanol; 1,2-dichloro-ethane; 1.1: Paal-Knorr reaction;
DOI:10.1021/ol102734g