2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

• Chemical Name: 2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
• CAS No.: 1082471-11-1
• Molecular Formula: C₂₄H₂₈N₄O₆
• Molecular Weight: 468.51

Synonyms:2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Chemical Property of 2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Technology Process of 2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 1 articles about 2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-azidoethyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside (186406-99-5) + benzyl bromide (100-39-0) → 2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside (1082471-11-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at -20 - 20 ℃;

DOI:10.1007/s11172-007-0258-y

Reference yield: 86.0%

2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside (1082471-11-1) → 2-azidoethyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside (1352813-64-9)

Guidance literature:

With water; acetic acid; at 40 ℃; for 36h;

DOI:10.1021/ja2083015

Reference yield: 84.0%

2-azidoethyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside (1082471-11-1) → 2-azidoethyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (1082470-89-0)

Guidance literature:

With trimethylamine-borane; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1007/s11172-007-0258-y

upstream raw materials:

2-azidoethyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

benzyl bromide

Downstream raw materials:

2-azidoethyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

2-azidoethyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

2-azidoethyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-tosyl-β-D-glucopyranoside

2-azidoethyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-β-D-glucopyranoside

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