C₄₉H₆₃N₁₃O₁₁

Base Information

Chemical Name:C₄₉H₆₃N₁₃O₁₁
CAS No.:1369573-37-4
Molecular Formula:C₄₉H₆₃N₁₃O₁₁
Molecular Weight:1010.12
Hs Code.:

C<sub>49</sub>H<sub>63</sub>N<sub>13</sub>O<sub>11</sub>

Synonyms:C₄₉H₆₃N₁₃O₁₁

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Chemical Property of C₄₉H₆₃N₁₃O₁₁

Chemical Property:

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Technology Process of C₄₉H₆₃N₁₃O₁₁

There total 17 articles about C₄₉H₆₃N₁₃O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₉H₆₅N₁₃O₁₂

: 1369573-37-4
C₄₉H₆₃N₁₃O₁₁

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 84520-68-3
N-tert-butoxycarbonyl-cis-4-azido-L-proline methyl ester

: 1369573-37-4
C₄₉H₆₃N₁₃O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

2.2: 25 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 20 °C

5.1: diethylamine / dichloromethane / 2 h / Cooling with ice

6.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

6.2: 48 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

9.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

10.1: sodium hydroxide / ethanol / 20 °C

10.2: pH 7

11.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 74844-91-0
1-tert-butyl 2-methyl (2S,4R)-4-hydroxy-1,2-pyrrolidinedicarboxylate

: 1369573-37-4
C₄₉H₆₃N₁₃O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine / 12 h / 0 - 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

4.2: 25 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24.67 h / 0 - 20 °C

7.1: sodium hydroxide / ethanol / 24 h / 20 °C

7.2: pH 4.5

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

9.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

10.1: sodium hydroxide / ethanol / 20 °C

10.2: pH 7

11.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With pyridine; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054