5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane

Base Information

Chemical Name:5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane
CAS No.:163852-37-7
Molecular Formula:C₄₂H₈₂PbS₄Si₆
Molecular Weight:1091.09
Hs Code.:

Synonyms:5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane

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Chemical Property of 5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane

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Technology Process of 5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane

There total 4 articles about 5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 10544-50-0
sulfur

: 241819-90-9
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(2,4,6-triisopropylphenyl)dibromoplumbane

: 163852-37-7
5-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiaplumbolane

Guidance literature:: With lithium naphthalenide; In tetrahydrofuran; Ar-atmosphere; LiNp addn. (-72°C); stirring (2 h); S8 addn. (-72°C); stirring (-72°C, 10 min; room temp., 10 min); filtration; filtrate concg. (vac.); gel permeation liq. chromy. (CHCl3);
DOI:10.1021/om990188z