9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

Base Information

Chemical Name:9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt
CAS No.:102212-64-6
Molecular Formula:C₁₈H₁₄N₅O₅*Na
Molecular Weight:403.329
Hs Code.:

Synonyms:9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

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Chemical Property of 9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

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Technology Process of 9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

There total 4 articles about 9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 102212-90-8
9-benzyl-1,3-dimethyl-7-<(N,N-dimethylamino)methenyl>-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione

: 102212-64-6
9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

Guidance literature:: With sodium hydroxide; 1.) 95-100 deg C, 75 min, 2.) RT, 23 h;
DOI:10.1021/jm00156a032

Reference yield:

: 57000-13-2
8-(benzylamino)-1,3-dimethyl-2,3,6,7-tetrahydro-1H-purine-2,6-dione

: 102212-64-6
9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / 9 h / 200 - 210 °C

2: 91 percent / POCl₃ / 22 h

3: 89 percent / 0.1 N NaOH / 1.) 95-100 deg C, 75 min, 2.) RT, 23 h

With sodium hydroxide; sodium methylate; trichlorophosphate;
DOI:10.1021/jm00156a032

Reference yield:

: 91285-01-7
9-benzyl-1,3-dimethyl-6-(hydroxy)pyrimido[2,1-f]purine-2,4,8(1H,3H,9H)-trione

: 102212-64-6
9-benzyl-1,3-dimethyl-7-formyl-6-hydroxypyrimido<2,1-f>purine-2,48(1H,3H,9H)-trione sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / POCl₃ / 22 h

2: 89 percent / 0.1 N NaOH / 1.) 95-100 deg C, 75 min, 2.) RT, 23 h

With sodium hydroxide; trichlorophosphate;
DOI:10.1021/jm00156a032