2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine

Base Information

• Chemical Name: 2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine
• CAS No.: 78763-66-3
• Molecular Formula: C₃₈H₂₉N₅O₈S
• Molecular Weight: 715.743

Synonyms:2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine

Chemical Property of 2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine

Chemical Property:

Purity/Quality:

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Technology Process of 2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine

There total 2 articles about 2'-O-(Thiobenzoyl)-N²,3'-O,5'-O-tribenzoylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethylbenzamide (611-74-5) → 2'-O-(Thiobenzoyl)-N2,3'-O,5'-O-tribenzoylguanosine (78763-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: phosgene / CH₂Cl₂

2: 2.) pyridine, H₂S / 1.) CH₂Cl₂, 24 h, 2.) 10 min

With pyridine; phosgene; hydrogen sulfide; In dichloromethane;

DOI:10.1021/jo00334a043

Reference yield:

N2,3'-O,5'-O-tribenzoylguanosine (62374-25-8) + N,N-dimethyl(chlorophenylmethylene)ammonium chloride (2397-26-4) → 2'-O-(Thiobenzoyl)-N2,3'-O,5'-O-tribenzoylguanosine (78763-66-3)

Guidance literature:

With pyridine; hydrogen sulfide; Yield given. Multistep reaction; 1.) CH₂Cl₂, 24 h, 2.) 10 min;

DOI:10.1021/jo00334a043

Reference yield: 85.0%

2'-O-(Thiobenzoyl)-N2,3'-O,5'-O-tribenzoylguanosine (78763-66-3) → N2,O3',O5'-tribenzoyl-2'-deoxyguanosine (78763-67-4)

Guidance literature:

With tri-n-butyl-tin hydride; In toluene; Heating;

DOI:10.1021/jo00334a043

upstream raw materials:

N²,3'-O,5'-O-tribenzoylguanosine

N,N-dimethyl(chlorophenylmethylene)ammonium chloride

N,N-dimethylbenzamide

Downstream raw materials:

N²,O^3',O^5'-tribenzoyl-2'-deoxyguanosine

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