N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide

Base Information

• Chemical Name: N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide
• CAS No.: 39964-89-1
• Molecular Formula: C₂₁H₂₉NO₇S
• Molecular Weight: 439.53

Synonyms:N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide

Chemical Property of N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide

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Technology Process of N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide

There total 7 articles about N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,4,5-trimethoxybenzyl bromide (21852-50-6) + N-(2,2-dimethoxyethyl)-p-toluenesulfonamide (58754-95-3) → N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide (39964-89-1)

Guidance literature:

N-(2,2-dimethoxyethyl)-p-toluenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; for 0.25h;

3,4,5-trimethoxybenzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Further stages.;

DOI:10.1021/ja0101072

Reference yield: 94.0%

N-(2'',2''-dimethoxyethyl)-3',4',5'-trimethoxyphenylmethylamine (54879-83-3) + p-toluenesulfonyl chloride (98-59-9) → N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide (39964-89-1)

Guidance literature:

With pyridine; for 72h; Ambient temperature;

Reference yield: 85.0%

5-(iodomethyl)-1,2,3-trimethoxybenzene (18111-18-7) + N-(2,2-dimethoxyethyl)-p-toluenesulfonamide (58754-95-3) → N-(2'',2''-dimethoxyethyl)-4-methyl-N-(3''',4''',5'''-trimethoxyphenylmethyl)benzene sulfonamide (39964-89-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 25 ℃; for 12h;

DOI:10.1016/S0040-4020(01)93272-7

upstream raw materials:

5-(iodomethyl)-1,2,3-trimethoxybenzene

N-(2,2-dimethoxyethyl)-p-toluenesulfonamide

3,4,5-trimethoxybenzyl bromide

N-(2'',2''-dimethoxyethyl)-3',4',5'-trimethoxyphenylmethylamine

Downstream raw materials:

5,6,7-trimethoxyisoquinoline

N-(2,2-dimethoxyethyl)-N-[(2-iodo-3,4,5-trimethoxyphenyl)methyl]-p-toluenesulfonamide

ethyl 2-benzoyl-1-cyano-8-ethoxycarbonyl-5,6,7-trimethoxy-1,2-dihydroisoquinoline-1-ethanoate

ethyl 2-benzoyl-1-cyano-5,6,7-trimethoxy-1-methyl-1,2-dihydroisoquinoline-8-carboxylate

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