N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

Base Information

Chemical Name:N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester
CAS No.:96866-20-5
Molecular Formula:C₂₄H₂₈N₂O₅
Molecular Weight:424.497
Hs Code.:

Synonyms:N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

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Chemical Property of N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

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Technology Process of N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

There total 4 articles about N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 87439-02-9
N-(3-carboxy-2-benzylidene-1-oxopropyl)glycine tert-butyl ester

: 96866-20-5
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 6456-74-2
Glycine tert-butyl ester

: 96866-20-5
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N,1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 83 percent / 1 N aq. NaOH / ethanol / 2 h / Ambient temperature

3: 67 percent / Et₃N,1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 87439-00-7
3-(ethoxycarbonyl)-2-benzylidenepropanoic acid

: 96866-20-5
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N,1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 83 percent / 1 N aq. NaOH / ethanol / 2 h / Ambient temperature

3: 67 percent / Et₃N,1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00147a007