methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

Base Information

Chemical Name:methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate
CAS No.:1345471-49-9
Molecular Formula:C₂₁H₁₉F₅O₄
Molecular Weight:430.371
Hs Code.:

Synonyms:methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

Chemical Property:

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Technology Process of methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

There total 3 articles about methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345471-44-4
1-bromo-4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}benzene

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1345471-49-9
methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

Guidance literature:: With palladium diacetate; In N,N-dimethyl-formamide;

Reference yield:

: 921623-31-6
4-(4,4,4-trifluorobutoxy)benzoic acid

: 1345471-49-9
methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: trifluorormethanesulfonic acid

2: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

3: palladium diacetate / N,N-dimethyl-formamide

With trifluorormethanesulfonic acid; bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

: 1345471-49-9
methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

2: palladium diacetate / N,N-dimethyl-formamide

With bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;