2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

Base Information

Chemical Name:2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate
CAS No.:1345471-42-2
Molecular Formula:CF₃O₃S*C₁₄H₁₆F₃OS₂
Molecular Weight:470.478
Hs Code.:

Synonyms:2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

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Chemical Property of 2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

There total 1 articles about 2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-80-8
1.3-propanedithiol

: 921623-31-6
4-(4,4,4-trifluorobutoxy)benzoic acid

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

Guidance literature:: With trifluorormethanesulfonic acid;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

: 73602-61-6,23588-89-8,29585-72-6,94527-74-9
triethylamine tris(hydrogen fluoride)

: 1345471-44-4
1-bromo-4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}benzene

Guidance literature:: With bromine; sodium hydrogencarbonate; triethylamine; In dichloromethane; ethyl acetate; toluene;

Reference yield:

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

: 1345472-51-6
2-(2,4-dinitrophenyl)ethyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]-methoxy}-phenyl)prop-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

2: palladium diacetate / N,N-dimethyl-formamide

3: 1,4-dioxane; water

4: dmap / dichloromethane; toluene; ethyl acetate

With dmap; bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;