5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

Base Information

Chemical Name:5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide
CAS No.:95015-77-3
Molecular Formula:C₂₂H₂₉N₃O₃
Molecular Weight:383.491
Hs Code.:

Synonyms:5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

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Chemical Property of 5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

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Technology Process of 5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

There total 6 articles about 5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 95015-83-1
Z-Tyr-Ava-PHA

: 95015-77-3
5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

Guidance literature:: With hydrogen; palladium; In methanol;
DOI:10.1248/cpb.32.4157

Reference yield:

: 16679-95-1
benzyl (S)-(1-hydrazinyl-3-(4-hydroxyphenyl)-1-oxopropan-2-yl)carbamate

: 95015-77-3
5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HNO₂ / DMF, azide method

2: 94 percent / hydrogen / Pd / methanol

With hydrogen; cis-nitrous acid; palladium; In methanol;
DOI:10.1248/cpb.32.4157

Reference yield:

: 23135-50-4
5-(N-benzyloxycarbonylamino)pentanoic acid

: 95015-77-3
5-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanoic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: THF, mixed anhydride method

2: hydrogen

3: 1.) HNO₂ / DMF, azide method

4: 94 percent / hydrogen / Pd / methanol

With hydrogen; cis-nitrous acid; palladium; In methanol;
DOI:10.1248/cpb.32.4157