1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

Base Information

Chemical Name:1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone
CAS No.:847373-45-9
Molecular Formula:C₅₄H₆₂N₈O₁₂
Molecular Weight:1015.13
Hs Code.:

Synonyms:1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

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Chemical Property of 1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

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Technology Process of 1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

There total 3 articles about 1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 199865-05-9
1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone

: 4114-31-2
ethylhydrazine carboxylate

: 847373-45-9
1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

Guidance literature:: With hydrogenchloride; In chloroform; Heating;
DOI:10.1002/jhet.5570410607

Reference yield:

: 15442-91-8
1,2,4,5-tetrabromomethylbenzene

: 847373-45-9
1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃; KI; Aliquat 336 / acetone / 48 h / Heating

2: 87 percent / aq. HCl / CHCl₃ / Heating

With hydrogenchloride; Aliquat 336; potassium carbonate; potassium iodide; In chloroform; acetone;
DOI:10.3390/10091126

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 847373-45-9
1-{4-[2,4,5-tri(4-acetylphenoxymethyl)benzyloxy]phenyl}-1-ethanone-N-ethoxycarbonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃; KI; Aliquat 336 / acetone / 48 h / Heating

2: 87 percent / aq. HCl / CHCl₃ / Heating

With hydrogenchloride; Aliquat 336; potassium carbonate; potassium iodide; In chloroform; acetone;
DOI:10.3390/10091126