2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

Base Information

Chemical Name:2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene
CAS No.:146132-84-5
Molecular Formula:C₂₁H₂₆O₅S
Molecular Weight:390.5
Hs Code.:

Synonyms:2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

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Chemical Property of 2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

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Technology Process of 2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

There total 3 articles about 2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-39-0
benzyl bromide

: 85576-26-7
mercaptobenzo<15-crown-5>

: 146132-84-5
2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

Guidance literature:: With sodium ethanolate; In ethanol;
DOI:10.1039/c39920001092

Reference yield:

: 14098-44-3
2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin

: 146132-84-5
2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / ClSO₃H / CHCl₃ / 0 °C

2: 83 percent / LiAlH₄ / tetrahydrofuran

3: 87 percent / NaOEt / ethanol

With chlorosulfonic acid; lithium aluminium tetrahydride; sodium ethanolate; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1039/c39920001092

Reference yield:

: 85576-25-6
(monobenzo-15-crown-5)-4'-sulphonyl chloride

: 146132-84-5
2-Benzylsulfanyl-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / LiAlH₄ / tetrahydrofuran

2: 87 percent / NaOEt / ethanol

With lithium aluminium tetrahydride; sodium ethanolate; In tetrahydrofuran; ethanol;
DOI:10.1039/c39920001092