methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

Base Information

Chemical Name:methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate
CAS No.:1452153-45-5
Molecular Formula:C₂₁H₁₈O₄
Molecular Weight:334.372
Hs Code.:

Synonyms:methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

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Chemical Property of methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

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Technology Process of methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

There total 3 articles about methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 83575-14-8
2-methoxycarbonyl-1,4-naphthoquinone

: 98-83-9,6144-04-3,25014-31-7,42612-14-6
isopropenylbenzene

: 1452153-45-5
methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

Guidance literature:: With ammonium cerium (IV) nitrate; In acetonitrile; at 20 ℃; for 0.333333h;
DOI:10.1039/c3ob40977e

Reference yield:

: 31519-22-9
1,4-dihydroxy-2-naphthoic acid

: 1452153-45-5
methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: silver(l) oxide; magnesium sulfate / diethyl ether / 16 h / 20 °C / Inert atmosphere

3: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 20 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; sodium hydrogencarbonate; magnesium sulfate; silver(l) oxide; In diethyl ether; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s00044-014-0929-9

Reference yield:

: 77060-74-3
methyl 1,4-dihydroxy-2-naphthoate

: 1452153-45-5
methyl 5-hydroxy-2-methyl-2-phenyl-2,3-dihydronaphtho[1,2-b]furan-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: silver(l) oxide; magnesium sulfate / diethyl ether / 16 h / 20 °C / Inert atmosphere

2: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 20 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; magnesium sulfate; silver(l) oxide; In diethyl ether; acetonitrile;
DOI:10.1007/s00044-014-0929-9