6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

Base Information

Chemical Name:6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine
CAS No.:168080-02-2
Molecular Formula:C₁₉H₁₆ClN₃O
Molecular Weight:337.809
Hs Code.:

Synonyms:6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

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Chemical Property of 6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

Chemical Property:

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Technology Process of 6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

There total 5 articles about 6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6,7-dihydro-5-(2-chloro-4-nitrobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

: 168080-02-2
6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; ethanol;

Reference yield:

: 33265-60-0
1-(2-nitrophenyl)-1H-pyrrole

: 168080-02-2
6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide / dimethyl sulfoxide

2: hydrogenchloride / ethanol

3: dimethylsulfide borane complex / tetrahydrofuran

4: triethylamine / dichloromethane

5: sodium hydroxide / tetrahydrofuran; ethanol

With hydrogenchloride; sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 63743-03-3
6,7-Dihydro-5H-pyrrolo[1,2-a][1,5]benzodiazepin-6-one

: 168080-02-2
6,7-Dihydro-5-(4-amino-2-chlorobenzoyl)-5H-pyrrolo[1,2-a][1,5]benzodiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran

2: triethylamine / dichloromethane

3: sodium hydroxide / tetrahydrofuran; ethanol

With sodium hydroxide; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;