C₁₅H₁₈O

Base Information

• Chemical Name: C₁₅H₁₈O
• CAS No.: 1432499-19-8
• Molecular Formula: C₁₅H₁₈O
• Molecular Weight: 214.307
• Mol file: 1432499-19-8.mol

Synonyms:C₁₅H₁₈O

Chemical Property of C₁₅H₁₈O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₈O

There total 3 articles about C₁₅H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenyl-5-hexenal (53847-17-9) + propargyl bromide (106-96-7) → C15H18O (1432499-19-8)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran; water; toluene; at 0 - 20 ℃; for 10h; Inert atmosphere;

DOI:10.1021/ja4025963

Reference yield:

2-phenylhex-5-enoic acid (156297-00-6) → C15H18O (1432499-19-8)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: zinc; ammonium chloride / toluene; water; tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; ammonium chloride; pyridinium chlorochromate; zinc; In tetrahydrofuran; dichloromethane; water; toluene;

DOI:10.1021/ja4025963

Reference yield:

2-phenyl-5-hexen-1-ol (177037-77-3) → C15H18O (1432499-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: zinc; ammonium chloride / toluene; water; tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere

With ammonium chloride; pyridinium chlorochromate; zinc; In tetrahydrofuran; dichloromethane; water; toluene;

DOI:10.1021/ja4025963

upstream raw materials:

2-phenyl-5-hexenal

propargyl bromide

2-phenylhex-5-enoic acid

2-phenyl-5-hexen-1-ol

Downstream raw materials:

C₁₅H₁₆O

C₁₅H₁₇ClO

C₁₅H₁₅ClO