N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

Base Information

Chemical Name:N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide
CAS No.:651055-61-7
Molecular Formula:C₂₅H₂₀N₄O₆S₂
Molecular Weight:536.589
Hs Code.:

Synonyms:N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

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Technology Process of N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

There total 4 articles about N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: N-(3-aminophenyl)-N'-(3-hydroxyphenyl)-9-oxo-9H-fluorene-2,7-disulfonamide

: 651055-61-7
N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

Guidance literature:: With pyridine; hydroxylamine hydrochloride; at 20 ℃; for 3h;

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 651055-61-7
N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1 h / 0 - 20 °C

2: sodium hydroxide; water / tetrahydrofuran; methanol / 24 h / Heating / reflux

3: pyridine; hydroxylamine hydrochloride / 3 h / 20 °C

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; water; In tetrahydrofuran; methanol;

Reference yield:

: 102-28-3
m-acetamide aniline

: 651055-61-7
N-(3-aminophenyl)-9-(hydroxyimino)-N'-(3-hydroxyphenyl)-9H-fluorene-2,7-disulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1 h / 0 - 20 °C

2: sodium hydroxide; water / tetrahydrofuran; methanol / 24 h / Heating / reflux

3: pyridine; hydroxylamine hydrochloride / 3 h / 20 °C

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; water; In tetrahydrofuran; methanol;