Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

Base Information

Chemical Name:Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester
CAS No.:498555-01-4
Molecular Formula:C₅₁H₇₆O₉
Molecular Weight:833.159
Hs Code.:

Synonyms:Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

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Chemical Property of Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

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Technology Process of Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

There total 5 articles about Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 498554-89-5
(1R,2S,3S,4R,6R)-2,3,4-Tris-benzyloxy-6-methoxy-cyclohexanol

: 498555-00-3
Imidazole-1-carboxylic acid (R)-2-methoxy-3-octadecyloxy-propyl ester

: 498555-01-4
Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; for 3h; Heating;
DOI:10.1021/ja0285159

Reference yield:

: 83167-59-3
1-O-octadecyl-2-O-methyl-sn-glycerol

: 498555-01-4
Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2 h / Heating

2: 84 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / Heating

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene;
DOI:10.1021/ja0285159

Reference yield:

: 162792-20-3
(1R,2R,3S,4S,5R)-3,4,5-Tris-benzyloxy-cyclohexane-1,2-diol

: 498555-01-4
Carbonic acid (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-methoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Bu₂SnO / toluene / 2 h / Heating

1.2: 90 percent / CsF / dimethylformamide / 20 °C

2.1: NaH / dimethylformamide / 1 h / 0 °C

3.1: 1.46 g / ceric ammonium nitrate / acetonitrile; H₂O / 0.33 h / 0 °C

4.1: 84 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3 h / Heating

With ammonium cerium(IV) nitrate; sodium hydride; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ja0285159