Fmoc-Phe-ψ(CSNH)-Gly-OH

Base Information

Chemical Name:Fmoc-Phe-ψ(CSNH)-Gly-OH
CAS No.:1070392-87-8
Molecular Formula:C₂₆H₂₄N₂O₄S
Molecular Weight:460.554
Hs Code.:

Synonyms:Fmoc-Phe-ψ(CSNH)-Gly-OH

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Chemical Property of Fmoc-Phe-ψ(CSNH)-Gly-OH

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Technology Process of Fmoc-Phe-ψ(CSNH)-Gly-OH

There total 3 articles about Fmoc-Phe-ψ(CSNH)-Gly-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 731806-50-1
Fmoc-PheΨ(CSNH)Gly-OBu^t

: 1070392-87-8
Fmoc-Phe-ψ(CSNH)-Gly-OH

Guidance literature:: With water; trifluoroacetic acid; for 1h;

Reference yield:

: Fmoc-L-Phe-Gly-OtBu

: 1070392-87-8
Fmoc-Phe-ψ(CSNH)-Gly-OH

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

2: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

With Lawessons reagent; triethylsilane; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1021/jo200497j

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1070392-87-8
Fmoc-Phe-ψ(CSNH)-Gly-OH

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

3: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

With Lawessons reagent; triethylsilane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1021/jo200497j